Nitroreductase activity of heart lipoamide dehydrogenase

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Nitroreductase activity of heart lipoamide dehydrogenase.

A novel reaction catalysed by lipoamide dehydrogenase is described. In the presence of NADH, lipoamide dehydrogenase reduces the nitro group of 4-nitropyridine and 4-nitropyridine N-oxide. The elution profiles from a DEAE-cellulose column for the dehydrogenase and nitroreductase activities are identical. Chemical modifications of critical amino acid residues suggest that the two activities shar...

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Lipoamide dehydrogenase from human liver.

Lipoamide dehydrogenase (reduced nicotinamide adenine dinucleotide :lipoamide oxidoreductase, EC 1.6.4.3) has been isolated from acid-precipitated human liver particles in a highly purified state by a freezing and thawing technique instead of the heat treatment used by other workers. The enzyme was found to have a molecular weight of 138,000, and to contain 2 moles of flavin adenine dinucleotid...

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Kinetics of Matrix-bound Lipoamide Dehydrogenase

Lipoamide dehydrogenase (EC 1.6.4.3) has been succesfully linked to a CNBr-activated polysaccharide matrix, Sepharose-4B, under different reaction conditions. The enzyme is probably bound more homogeneously at lower pH values (pH 7.5) than at pH 8.5. Such immobilized preparations yield V values 8 — 30% of the value of the V of the free enzyme (18,600 mole/min/mole of flavin). A low level of CNB...

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Lipoamide dehydrogenase in serum: a preliminary report.

Lipoamide dehydrogenase was identified in serum and the optimal conditions for its assay at 30 degrees C were defined. The pH optimum in tris(hydroxymethyl)aminomethane buffer is 7.8, and activity is inhibited if buffer concentration exceeds 100 mmol/liter. Saturating concentrations of the substrates NAD+ and lipoamide are 3 mmol/liter and 5 mmol/liter, respectively. Activity is decreased eight...

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NADH inhibition and NAD activation of Escherichia coli lipoamide dehydrogenase catalyzing the NADH-lipoamide reaction.

A unique form of inhibition by NADH and partial reversal by NAD+ has been demonstrated with Escherichia coli lipoamide dehydrogenase. Substrate inhibition by NADH is consistent with its reduction of the active two-electron reduced enzyme intermediate to the inactive four-electron reduced form. NAD+ partially overcomes this inhibition by mass action reversal of this reduction. NAD+ activation is...

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ژورنال

عنوان ژورنال: Biochemical Journal

سال: 1987

ISSN: 0264-6021,1470-8728

DOI: 10.1042/bj2420447